03/12/2021
ANALYZER SAMPLE SYSTEMS
Some analyzers measure the composition of a process stream by directly immersing the sensing element in that stream. This is called in situ measurement, which is a Latin phrase meaning “in the place.”
A pH probe inserted into a process pipe, an oxygen probe inserted into the stack of a combustion furnace, and a GFC analyzer measuring the concentration of a gaseous pollutant by shooting a light beam across a process room are all examples of in situ analyzers: the analytical sensing takes place directly within the process environment.
Alternatively, analytical sensing elements may be located some distance away from the process, in which case a representative sample of that process stream must be conveyed to the analyzer for measurement. A great many industrial analyzers function like this, with a system of tubes, heaters, filters, pumps, regulators, and other components working together to provide the remotely located analyzer with a steady stream of process fluid to sample. It should be noted that quite often problems experienced with process analyzers stem from improperly constructed and/or maintained sample systems.
A very simple sample system for a pH analyzer is shown here, the purpose for it being to allow the pH electrode to operate at atmospheric pressure instead of the high pressure inside the process pipe (Note):
Note : In-situ pH probes are manufactured for high-pressure applications, but they suffer short lifespans (due to the accelerated erosion of the measurement glass) and decreased sensitivity (due to the extra thickness of the measurement glass) and are substantially more expensive than pH probes designed for atmospheric pressure conditions.
Liquid from the process pipe flows through the isolation and flow-control valves, the rate of flow restricted to a mere trickle, where it continuously fills a sample chamber and overflows into a process sewer designed to transport a constant stream of process liquid. If for some reason a process sewer drain is unsafe, environmentally destructive, or impractical, one may replace the overflow tube with a level control system and pump to re-inject the sample back into the process line. This, of course, adds complexity and expense to the sample system.
Credit: Instruments Tools
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